An Efficient and One Spot Synthesis of Silica Supported Synthesis of Fluorinated 1,3,4-Thiadiazole Derivative Under Microwave Irradiation

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Authors

  • Bharat K Dhotre Swami Vivekanand Senior College, Mantha, Jalna, Maharashtra, India
  • Bhagwan Singh Dobhalb Badrinarayan Barwale Mahavidyalaya, Jalna, India
  • Santosh Raut Maulana Azad College, Aurangabad, Maharashtra, India
  • Amol Kalea Swami Vivekanand Senior College, Mantha, Jalna, Maharashtra, India
  • Pathan Mohd Arif Maulana Azad College, Aurangabad, Maharashtra, India

Keywords:

Microwave irradiation, Silica supported, thiosemicarbazide

Abstract

An efficient and one pot reaction of fluorinated 1,3,4-Thiadiazole derivatives  was synthesis by fluorinated  aromatic carboxylic with thiosemicabazide in the presence of phosphorus oxychloride as a catalyst under Microwave irradiation with silica supported. The synthesis compound was characterized by 1H NMR, IR, and mass spectroscopic techniques. The present approach offers the advantages such as short reaction time, simplicity of the workup procedure, low cost and mild reaction condition.

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Author Biographies

Bharat K Dhotre, Swami Vivekanand Senior College, Mantha, Jalna, Maharashtra, India

Department of Chemistry

Bhagwan Singh Dobhalb, Badrinarayan Barwale Mahavidyalaya, Jalna, India

Department of Chemistry

Santosh Raut, Maulana Azad College, Aurangabad, Maharashtra, India

Department of Chemistry

Amol Kalea, Swami Vivekanand Senior College, Mantha, Jalna, Maharashtra, India

Department of Chemistry 

Pathan Mohd Arif , Maulana Azad College, Aurangabad, Maharashtra, India

  Department of Chemistry

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Published

2020-06-13

How to Cite

Bharat K Dhotre, Bhagwan Singh Dobhalb, Santosh Raut, Amol Kalea, & Pathan Mohd Arif. (2020). An Efficient and One Spot Synthesis of Silica Supported Synthesis of Fluorinated 1,3,4-Thiadiazole Derivative Under Microwave Irradiation: -. To Chemistry Journal, 6, 61-65. Retrieved from https://purkh.com/index.php/tochem/article/view/789

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Research Articles